反应详情

A solution of 3,4-difluorothiophenol (3 g), ethyl iodide (1.6 ml), potassium carbonate (2.64 g) and DMF (40 ml) were charged to a flask and stirred for 2 h. The solution was partitioned between ethyl acetate and water. The organic extracts were dried (MgSO4) and evaporated under reduced pressure to give the subtitle compound (3.84 g).

1. customThe solution was partitioned between ethyl acetate and water
2. dry with materialThe organic extracts were dried (MgSO4)
3. customevaporated under reduced pressure