HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 67264048, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 4-Nitro-isatoic anhydride | HCID 282089 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 67264048 | HCID 67264048 | — |
Reaction Steps
7-Nitro-1H-3,1-benzoxazine-2,4-dione (1.14 g, 0.00549 mol) was dissolved in THF (50 mL, 0.6 mol). 2 M of Methylamine in THF (10 mL) was added, and a yellow solid formed immediately. The reaction mixture was concentrated under reduced pressure to afford a light orange solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08148391B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-5490aeb9ffa549e19adc97176d7f67f3 |
| Source note | uspto-grants-2012_04 |