反应详情

7-Nitro-1H-3,1-benzoxazine-2,4-dione (1.14 g, 0.00549 mol) was dissolved in THF (50 mL, 0.6 mol). 2 M of Methylamine in THF (10 mL) was added, and a yellow solid formed immediately. The reaction mixture was concentrated under reduced pressure to afford a light orange solid.

1. customa yellow solid formed immediately
2. concentrationThe reaction mixture was concentrated under reduced pressure
3. customto afford a light orange solid