Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 62691367 | HCID 62691367 | — |
| Product | HCID 67263938 | HCID 67263938 | — |
Reaction Steps
8 M of H2O2 in Water (4.4 mL) was added to a solution of 1-Fluoro-3-isopropylsulfanyl-2-nitro-benzene (6.76 g, 0.031 mol) in Acetic acid (10 mL, 0.2 mol), and the reaction was heated at 100° C. for 16 h HPLC. Addition 2.5 eq H2O2 added. The reaction mixture was cooled and added to ice, when the product precipitated, and was collected by filtration, washed with water and dried under vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08148391B2 |
|---|
| Source dataset | uspto-grants-2012_04 |
|---|
| ORD ID | ord-e9e65266d85946b2b281038f99960d49 |
|---|
| Source note | uspto-grants-2012_04 |
|---|
