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HRID1687634

反应详情

EQUATION

反应方程式

HRID 1687634 的结构方程式

REACTANTS

反应物

3
结构：CN(C)C=O
HCID6228

N,N-Dimethylformamide

C3H7NO

结构：[N-]=[N+]=[N-].[Na+]
HCID33557

未命名化合物

结构：CC1(C)CC(I)C(=O)Nc2cc([N+](=O)[O-])ccc21
HCID67264356

未命名化合物

PRODUCTS

生成物

1
结构：CC1(C)CC(N=[N+]=[N-])C(=O)Nc2cc([N+](=O)[O-])ccc21
HCID86633991

未命名化合物

PROCEDURE

实验过程

3-Iodo-5,5-dimethyl-8-nitro-1,3,4,5-tetrahydro-1-benzazepin-2-one (5.367 g, 0.015 mol), Sodium azide (6.49 g, 0.1 mol), and DMF (100 mL, 2 mol) were stirred at rt for 2 h. The reaction mixture was diluted with H20 and the resulting beige ppt was filtered.

WORKUP

后处理

  1. additionThe reaction mixture was diluted with H20
  2. filtrationthe resulting beige ppt was filtered