HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 86654369, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 66907575 | HCID 66907575 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86654369 | HCID 86654369 | — |
Reaction Steps
1.2 g (0.0054 mol) of the compound 2d) from the previous step, 20 ml of dichloromethane, 0.75 ml (0.0054 mol) of triethylamine and, at 0-5° C., 0.42 ml (0.0054 mol) of methanesulfonyl chloride are placed in a round-bottom flask.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08153637B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-b750f0d0269544398bbf95644a411b2e |
| Source note | uspto-grants-2012_04 |