Hydrochloric Acid → HCID 24855045, compound

Participants

Reaction Steps

A mixture of 3-[4-(2-fluoro-pyridin-4-yl)-thieno[3,2-d]pyrimidin-2-yl]-phenol, (60 mg), aqueous HCl (2M, 2 mL) and 1,4-dioxane (2 mL) was heated to reflux for 24 hours. Upon cooling, a precipitate formed; this was collected by filtration and washed with water and ether to yield the furnish the title compound (50 mg).

Provenance & Evidence