HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(3-Azabicyclo[3.2.0]hept-3-yl)-5-nitropyridine → 6-(3-Azabicyclo[3.2.0]hept-3-yl)-3-aminopyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(3-Azabicyclo[3.2.0]hept-3-yl)-5-nitropyridine | HCID 66907896 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 6-(3-Azabicyclo[3.2.0]hept-3-yl)-3-aminopyridine | HCID 59190089 | 92.2% |
Reaction Steps
According to a procedure similar to that described in Stage 14.2, starting from 0.12 g (0.55 mmol) of 2-(3-azabicyclo[3.2.0]hept-3-yl)-5-nitropyridine, prepared in the preceding stage, and 0.17 g of palladium on charcoal at 10%, we obtain 0.096 g of the expected compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08153650B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-7b60695ef7f847f5a3c2790698bd76eb |
| Source note | uspto-grants-2012_04 |