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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1690513Erstellt: 25. Oktober 2026

2,6-Xylyl isocyanate → 1-Cyclohexyl-3-(2,6-dimethyl-phenyl)-1-(2-phenyl-2H-indazol-3-yl)-urea

https://huagongshe.com/reaction/1690513

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt2,6-Xylyl isocyanateHCID 98787—
EduktN-Cyclohexyl-2-phenyl-2H-indazol-3-amineHCID 12318206—
LösungsmittelTolueneHCID 1140—
Produkt1-Cyclohexyl-3-(2,6-dimethyl-phenyl)-1-(2-phenyl-2H-indazol-3-yl)-ureaHCID 45110617—

Reaktionsschritte

In analogy to the procedure described in example 1.2, cyclohexyl-(2-phenyl-2H-indazol-3-yl)-amine (example 1.1) was reacted with 2-isocyanato-1,3-dimethyl-benzene ([28556-81-2]) in toluene for 72 h under reflux conditions to give the title compound as yellow oil. MS: m/e=439.3 [M+H+].

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08153663B2
Quelldatensatzuspto-grants-2012_04
ORD IDord-a03121c44e3149f7b2a0a96fa6ca83bd
Quellennotizuspto-grants-2012_04