HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2,6-Xylyl isocyanate → 1-Cyclohexyl-3-(2,6-dimethyl-phenyl)-1-(2-phenyl-2H-indazol-3-yl)-urea
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2,6-Xylyl isocyanate | HCID 98787 | — |
| Edukt | N-Cyclohexyl-2-phenyl-2H-indazol-3-amine | HCID 12318206 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | 1-Cyclohexyl-3-(2,6-dimethyl-phenyl)-1-(2-phenyl-2H-indazol-3-yl)-urea | HCID 45110617 | — |
Reaktionsschritte
In analogy to the procedure described in example 1.2, cyclohexyl-(2-phenyl-2H-indazol-3-yl)-amine (example 1.1) was reacted with 2-isocyanato-1,3-dimethyl-benzene ([28556-81-2]) in toluene for 72 h under reflux conditions to give the title compound as yellow oil. MS: m/e=439.3 [M+H+].
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08153663B2 |
| Quelldatensatz | uspto-grants-2012_04 |
| ORD ID | ord-a03121c44e3149f7b2a0a96fa6ca83bd |
| Quellennotiz | uspto-grants-2012_04 |