HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-isocyanatobenzoate → HCID 66905646, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-isocyanatobenzoate | HCID 589806 | — |
| Reactant | N-Cyclohexyl-2-phenyl-2H-indazol-3-amine | HCID 12318206 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 66905646 | HCID 66905646 | — |
Reaction Steps
In analogy to the procedure described in example 1.2, cyclohexyl-(2-phenyl-2H-indazol-3-yl)-amine (example 1.1) was reacted with 3-isocyanato-benzoic acid ethyl ester ([41221-47-0]) in toluene for 72 h under reflux conditions to give the title compound as yellow oil. MS: m/e=469.3 [M+H+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08153663B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-97e643c263284e2dba5cd3e172f51b61 |
| Source note | uspto-grants-2012_04 |