HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexylamine → HCID 66905291, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | HCID 66905406 | HCID 66905406 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 66905291 | HCID 66905291 | — |
Reaction Steps
In analogy to the procedure described in example 4.1, 3-chloro-2-(4-chloro-phenyl)-6-fluoro-2H-indazole was reacted with cyclohexylamine ([108-91-8]) in N-methyl 2-pyrrolidone for 72 h at 150° C. in a sealed tube to give the title compound as yellow solid. MS: m/e=344.5 [M+H+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08153663B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-7f8d712f298942029a39bc050cfe3e5f |
| Source note | uspto-grants-2012_04 |