HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodine → HCID 66905241, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodine | HCID 807 | — |
| Reactant | 3-Chloroaniline | HCID 7932 | — |
| Reactant | Sodium Sulfate | HCID 24436 | — |
| Reactant | Indium | HCID 5359967 | — |
| Reactant | 4,5-Difluoro-2-nitrobenzaldehyde | HCID 19957297 | — |
| Product | HCID 66905241 | HCID 66905241 | — |
Reaction Steps
In analogy to the procedure described in example 35.1, 3-chloroaniline was reacted with 4,5-difluoro-2-nitro-benzaldehyde (Daubie, Christophe; Legrand, Jean Jacques; Pemberton, Clive. Eur. Pat. Appl. (1993), EP 538 100 A1) in the presence of Na2SO4, indium and iodine to give the title compound as brown solid. MS: m/e=388.0 [M−H−].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08153663B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-ba2caa7f8b814ad6ae99aef1338a3e6c |
| Source note | uspto-grants-2012_04 |