HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloroaniline → HCID 66905477, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloroaniline | HCID 7932 | — |
| Reactant | HCID 66905406 | HCID 66905406 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 66905477 | HCID 66905477 | — |
Reaction Steps
In analogy to the procedure described in example 4.1, 3-chloro-2-(4-chloro-phenyl)-6-fluoro-2H-indazole (example 40.2) was reacted with 3-chloro-phenylamine ([108-42-9]) in N-methyl 2-pyrrolidone for 72 h at 175° C. in a sealed tube to give the title compound as colorless crystals. MS: m/e=372.1 [M+H+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08153663B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-f6bc1cde18af4234a384b61fa499fba2 |
| Source note | uspto-grants-2012_04 |