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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1690603Generated: November 3, 2026

Triethylamine → HCID 66905435, compound

https://huagongshe.com/reaction/1690603

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
ReactantHCID 45111767HCID 45111767—
Reactant3-Chloro-4-isocyanato-benzoic acid methyl esterHCID 86640262—
Solvent1,2-DichloroethaneHCID 11—
ProductHCID 66905435HCID 66905435—

Reaction Steps

In analogy to the procedure described in example 1.2, cyclohexyl-(2-phenyl-4,5,6,7-tetrahydro-2H-indazol-3-yl)-amine (example 45) was reacted with 3-chloro-4-isocyanato-benzoic acid methyl ester (example 9.1) in 1,2-dichloroethane in the presence of triethylamine for 120 h under reflux conditions to give the title compound as yellow solid. MS: m/e=507.2 [M+H+].

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08153663B2
Source datasetuspto-grants-2012_04
ORD IDord-e5e066c357ed47608b236815e601be83
Source noteuspto-grants-2012_04