HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 66905435, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 45111767 | HCID 45111767 | — |
| Reactant | 3-Chloro-4-isocyanato-benzoic acid methyl ester | HCID 86640262 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 66905435 | HCID 66905435 | — |
Reaction Steps
In analogy to the procedure described in example 1.2, cyclohexyl-(2-phenyl-4,5,6,7-tetrahydro-2H-indazol-3-yl)-amine (example 45) was reacted with 3-chloro-4-isocyanato-benzoic acid methyl ester (example 9.1) in 1,2-dichloroethane in the presence of triethylamine for 120 h under reflux conditions to give the title compound as yellow solid. MS: m/e=507.2 [M+H+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08153663B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-e5e066c357ed47608b236815e601be83 |
| Source note | uspto-grants-2012_04 |