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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1690843Generated: October 31, 2026

Ethyl Acetate → HCID 24991587, compound

https://huagongshe.com/reaction/1690843

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthyl AcetateHCID 8857—
ReactantHCID 66906071HCID 66906071—
SolventHexaneHCID 8058—
ProductHCID 24991587HCID 24991587—

Reaction Steps

This ester was prepared using the procedure described in Example 5, except 2-(2-chlorophenyl)-3-hydroxypropanenitrile was used in place of 2-2-chloro-5-(difluoromethoxy)phenyl-3-hydroxypropanenitrile. The preparation of 2-(2-chlorophenyl)-3-hydroxypropanenitrile is described in Example 13. The recovered ester product was a colorless oil (70% yield), Rf 0.3 (silica gel, ethyl acetate:hexane=1:4).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08153688B2
Source datasetuspto-grants-2012_04
ORD IDord-863dff0948dc4e599b75a71927d31595
Source noteuspto-grants-2012_04