HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 66906227, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 13558941 | HCID 13558941 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 66906227 | HCID 66906227 | 86% |
Reaction Steps
A 175 mg (0.738 mmol) sample of the above 3-hydroxy-2-(3-phenoxyphenyl)propanenitrile was acylated with acetic anhydride (74 μL) in acetonitrile (300 μL) using the procedure described in Example 5 to give 147 mg (86% yield) of 3-acetoxy-2-(3-phenoxyphenyl)propanenitrile as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08153688B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-5d8efaf9f1c44cfaa8d660e6c492ee8f |
| Source note | uspto-grants-2012_04 |