HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Hydroxy-4-nitrobenzyl alcohol → 2-Hydroxy-4-nitrobenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Hydroxy-4-nitrobenzyl alcohol | HCID 11816094 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 2-Hydroxy-4-nitrobenzaldehyde | HCID 75570 | — |
Reaction Steps
6.0 g (35.5 mmol) of 2-(hydroxymethyl)-5-nitrophenol and 3.1 g (35.5 mmol) of activated manganese(IV) oxide in 100 ml of chloroform are heated under reflux for 20 h. The mixture is filtered through kieselguhr, concentrated and dried under high vacuum. The title compound is immediately reacted further.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08153799B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-fb9b9904369d4cc5a61f7be55577c6e1 |
| Source note | uspto-grants-2012_04 |