HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-2-isocyanato-4-methoxy-5-methyl-benzene → 4-oxo-3,4-dihydro-2H-[2,3']bipyridinyl-1-carboxylic acid (2-bromo-5-methoxy-4-methyl-phenyl)-amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-2-isocyanato-4-methoxy-5-methyl-benzene | HCID 59377751 | — |
| Reactant | 2,3-dihydro-1H-[2,3']bipyridinyl-4-one | HCID 59377784 | — |
| Product | 4-oxo-3,4-dihydro-2H-[2,3']bipyridinyl-1-carboxylic acid (2-bromo-5-methoxy-4-methyl-phenyl)-amide | HCID 59377804 | — |
Reaction Steps
2,3-Dihydro-1H-[2,3′]bipyridinyl-4-one was reacted with 1-bromo-2-isocyanato-4-methoxy-5-methyl-benzene using the procedure of step 3 of Example 1 to afford 4-oxo-3,4-dihydro-2H-[2,3′]bipyridinyl-1-carboxylic acid (2-bromo-5-methoxy-4-methyl-phenyl)-amide, MS (M+H) 417.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08153809B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-155a9b925ab84cc18b31bfcce713c943 |
| Source note | uspto-grants-2012_04 |