HRID1692628

反应详情

EQUATION

反应方程式

HRID 1692628 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a stirring solution of psoromic acid (1 mmol) in ethanol (25 mL) was added hydrazine hydrate (1 mmol). The reaction was stirred for half an hour and monitored by TLC. Upon completion, all of the solvent was removed by rotary evaporation. The residue was redissolved in ethanol and dried over anhydrous magnesium sulfate, filtered, and evaporated by a rotary evaporator to yield a white solid product.

WORKUP

后处理

  1. customUpon completion, all of the solvent was removed by rotary evaporation
  2. dissolutionThe residue was redissolved in ethanol
  3. dry with materialdried over anhydrous magnesium sulfate
  4. filtrationfiltered
  5. customevaporated by a rotary evaporator
  6. customto yield a white solid product