HRID1692628
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To a stirring solution of psoromic acid (1 mmol) in ethanol (25 mL) was added hydrazine hydrate (1 mmol). The reaction was stirred for half an hour and monitored by TLC. Upon completion, all of the solvent was removed by rotary evaporation. The residue was redissolved in ethanol and dried over anhydrous magnesium sulfate, filtered, and evaporated by a rotary evaporator to yield a white solid product.
WORKUP
后处理
- customUpon completion, all of the solvent was removed by rotary evaporation
- dissolutionThe residue was redissolved in ethanol
- dry with materialdried over anhydrous magnesium sulfate
- filtrationfiltered
- customevaporated by a rotary evaporator
- customto yield a white solid product