HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Benzyloxy-phenoxy)-benzoic acid benzyl ester → 2-(2-Hydroxyphenoxy)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Benzyloxy-phenoxy)-benzoic acid benzyl ester | HCID 67280358 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-(2-Hydroxyphenoxy)benzoic acid | HCID 611388 | — |
Reaction Steps
2-(2-Benzyloxy-phenoxy)-benzoic acid benzyl ester (440 mg, 1 mmol) was dissolved in ethanol (30 mL), and 10% palladium on carbon (44 mg) was added. The mixture was stirred overnight under nitrogen protection. The suspension was filtered, evaporated by a rotatory evaporator to produce 2-(2-hydroxy-phenoxy)-benzoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08158623B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-53784206bed64b3282dace63542f0e17 |
| Source note | uspto-grants-2012_04 |