HRID1692763

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6422

未命名化合物

结构：CN(C(=O)OC(C)(C)C)c1ccc(B2OC(C)(C)C(C)(C)O2)cn1

HCID44541676

tert-Butyl methyl[5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-yl]carbamate

C17H27BN2O4

HCID86630067

未命名化合物

PRODUCTS

生成物

结构：CNc1ccc(-c2nc(N3CCOCC3)c3nc(C(C)(C)OC)sc3n2)cn1

HCID25253836

未命名化合物

PROCEDURE

实验过程

Crude 4-(5-chloro-2-(2-methoxypropan-2-yl)thiazolo[5,4-d]pyrimidin-7-yl)morpholine (60 mg) was reacted with tert-butyl methyl(5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-yl)carbamate via general procedure A. This crude product was then treated with TFA to remove residual protecting group and purified via reverse phase HPLC to get 58.4 mg 102. MS (Q1) 401.2 (M)+.

WORKUP

后处理

customto remove residual
custompurified via reverse phase HPLC