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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1693059Generated: November 3, 2026

Hydrochloric Acid → HCID 57458146, compound

https://huagongshe.com/reaction/1693059

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 67279159HCID 67279159—
SolventMethanolHCID 887—
ProductHCID 57458146HCID 57458146—

Reaction Steps

To ((R)—N—((R)-1-(2-chloro-4-methoxy-5-methylphenyl)ethyl)-2-methylpropane-2-sulfinamide (0.64 g, 2.1 mmol) was added 10% hydrogen chloride in methanol (10 ml), and the resulting mixture was stirred at room temperature for 3 h. The reaction mixture was evaporated and dried in vacuo to give the title compound (crude 0.63 g) as white solid. This amine was used for the next step without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08158650B2
Source datasetuspto-grants-2012_04
ORD IDord-902e8a70ebd04bb8bd252bfd4961c2db
Source noteuspto-grants-2012_04