HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 57458146, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 67279159 | HCID 67279159 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57458146 | HCID 57458146 | — |
Reaction Steps
To ((R)—N—((R)-1-(2-chloro-4-methoxy-5-methylphenyl)ethyl)-2-methylpropane-2-sulfinamide (0.64 g, 2.1 mmol) was added 10% hydrogen chloride in methanol (10 ml), and the resulting mixture was stirred at room temperature for 3 h. The reaction mixture was evaporated and dried in vacuo to give the title compound (crude 0.63 g) as white solid. This amine was used for the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08158650B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-902e8a70ebd04bb8bd252bfd4961c2db |
| Source note | uspto-grants-2012_04 |