HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Fluoro-3-methylbenzo[b]thiophene-2-sulphonyl chloride → HCID 59759963, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Fluoro-3-methylbenzo[b]thiophene-2-sulphonyl chloride | HCID 2774586 | — |
| Reactant | 4-Bromo-2-ethylaniline | HCID 2801283 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 59759963 | HCID 59759963 | 46.6% |
Reaction Steps
This compound was prepared in analogy to Example 1, starting from 4-bromo-2-ethylaniline (CAS:45762-41-2, 2.0 g) and 5-fluoro-3-methylbenzo[b]thiophene-2-sulphonyl chloride (0.265 g) in pyridine (2.0 ml) for 4 h to obtain the desired compound (0.20 g) as a colorless solid. MS (ISP): 445.0, 447.0 (M+NH4)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08158655B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-36b00e917fa641559f85449afd0c9ec9 |
| Source note | uspto-grants-2012_04 |