Sodium hydride → HCID 24966676, compound

Participants

Reaction Steps

This compound was prepared in analogy to Example 20f starting from 2-methanesulfonyl-4-pyridin-4-yl-phenylamine (cf. Example 20c, 0.27 g) in tetrahydrofurane (10 ml) and 5-fluoro-3-methylbenzo[b]thiophene-2-sulphonyl chloride (0.265 g) with sodium hydride (0.10 g) at rt for 18 h to obtain the title compound (0.025 g) as a yellow foam. MS (ISN): 475.0 (M−H)−

Provenance & Evidence