HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen chloride-ethyl acetate → HCID 67280993, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Reactant | HCID 59759984 | HCID 59759984 | — |
| Product | HCID 67280993 | HCID 67280993 | — |
Reaction Steps
This compound was prepared in analogy to example 27b starting from 5-fluoro-3-methyl-2-(4-pyridin-4-yl-2-trifluoromethyl-phenylsulfamoyl)-indole-1-carboxylic acid tert-butyl ester (0.052 g), 2.5 N HCl/ethyl acetate (10.0 ml) to obtain the title compound (0.041 g) as a brownish amorphous powder. MS (ISN): 448.4 (M−H)−
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08158655B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-bb3adfc703db421a92d245e88f37ee69 |
| Source note | uspto-grants-2012_04 |