HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2-(trifluoromethyl)aniline → HCID 59759973, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2-(trifluoromethyl)aniline | HCID 67960 | — |
| Reactant | HCID 59759982 | HCID 59759982 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 59759973 | HCID 59759973 | 65.9% |
Reaction Steps
This compound was prepared in analogy to Example 1 starting from 5-fluoro-1,3-dimethyl-1H-indole-2-sulfonyl chloride (0.25 g) and 2-amino-5-bromobenzotrifluoride (2.3 g) in pyridine (5 ml) for 18 h at 35° C. to obtain the title compound (0.293 g) as a yellow solid. MS (ISN): 551.4, 549.3 (M−H)−
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08158655B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-c3c6e5fba4ba417b8a0c3fd3bf0c5625 |
| Source note | uspto-grants-2012_04 |