HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86641350, compound → HCID 67280852, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86641350 | HCID 86641350 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 67280852 | HCID 67280852 | 32% |
Reaction Steps
Synthesis was performed by the same method as in Example 111 using the above tert-butyl {8-[2-(ethylamino)ethyl]-2-[(4-methoxy-3,5-dimethylpyridin-2-yl)methyl]-2,7-dihydro-6-thia-1,2,3,5-tetraazabenzo[cd]azulen-4-yl}carbamate (17 mg), followed by trituration with diethyl ether to obtain the title compound (4.4 mg, 31%) as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08158638B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-0e96657a1fac42a9ba59d57337e1618b |
| Source note | uspto-grants-2012_04 |