HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Ethanediamine, N1-phenyl- → 1H-Pyrrolo[2,3-c]pyridine-2-carboxylic acid (2-phenylaminoethyl)amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Ethanediamine, N1-phenyl- | HCID 74270 | — |
| Reactant | 1H-Pyrrolo(2,3-c)pyridine-2-carboxylic acid | HCID 21819002 | — |
| Product | 1H-Pyrrolo[2,3-c]pyridine-2-carboxylic acid (2-phenylaminoethyl)amide | HCID 11737579 | — |
Reaction Steps
The title compound was prepared as outlined in EXAMPLE 1 from 1H-pyrrolo[2,3-c]pyridine-2-carboxylic acid (Preparation 15) and 2-phenylaminoethylamine to give the title compound as a pale yellow solid. δH (CD3OD): 3.37 (2H, t), 3.63 (2H, t), 6.61 (1H, t), 6.69 (2H, d), 7.08-7.13 (2H, m), 7.64 (1H, d), 8.10 (1H, d), 8.78 (1H, s); m/z (ES+)=281 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08158622B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-ed9b6c1ab41b4e9ba162fc1e69e79d26 |
| Source note | uspto-grants-2012_04 |