HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Benzylpiperazin-1-yl)ethan-1-amine → 5-Chloro-1H-pyrrolo[2,3-c]pyridine-2-carboxylic acid [2-(4-benzylpiperazin-1-yl)ethyl]amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Benzylpiperazin-1-yl)ethan-1-amine | HCID 2735331 | — |
| Reactant | 5-chloro-1H-pyrrolo[2,3-c]pyridine-2-carboxylic acid | HCID 44630704 | — |
| Product | 5-Chloro-1H-pyrrolo[2,3-c]pyridine-2-carboxylic acid [2-(4-benzylpiperazin-1-yl)ethyl]amide | HCID 11749879 | — |
Reaction Steps
The title compound was prepared as outlined in EXAMPLE 1 from 5-chloro-1H-pyrrolo[2,3-c]pyridine-2-carboxylic acid (Preparation 18) and 4-benzylpiperazin-1 ylethylamine. The product was purified by mass directed purification to give the title compound as an orange solid. m/z (ES+)=398 [M+H]+; RT=2.75 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08158622B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-393ff36ea8bb4c8b81d77170f3299917 |
| Source note | uspto-grants-2012_04 |