HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethylpiperidin-4-amine → HCID 59753594, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethylpiperidin-4-amine | HCID 417391 | — |
| Reactant | 2-(S)-[(5-Chloro-1H-pyrrolo[2,3-c]pyridine-2-carbonyl)amino]-3-(4-fluorophenyl)propionic acid | HCID 59753699 | — |
| Product | HCID 59753594 | HCID 59753594 | — |
Reaction Steps
The title compound was prepared according to EXAMPLE 35 from 2-(S)-[(5-chloro-1H-pyrrolo[2,3-c]pyridine-2-carbonyl)amino]-3-(4-fluorophenyl)propionic acid (EXAMPLE 228) and dimethylpiperidin-4-yl amine (Preparation 90). Purification by preparative HPLC gave the title compound as a yellow crystalline solid. m/z (ES+)=472.34 [M+H]+; RT=2.64 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08158622B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-ce060b87c3494775b70cf13c025a2e01 |
| Source note | uspto-grants-2012_04 |