HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Isothiocyanate → HCID 11666764, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Isothiocyanate | HCID 2346 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Phenethyl isocyanate | HCID 160602 | — |
| Product | HCID 11666764 | HCID 11666764 | — |
Reaction Steps
Reagents: Benzyl-isothiocyanate (6.5 mmol, 0.85 mL), phenethylisocyanate (6.5 mmol, 0.89 mL) and SO2Cl2 (6.5 mmol, 0.52 mL) in diethyl ether (25 mL). Isolation: solvent evaporation. Purification: silica gel column chromatography (AcOEt/hexane, 1:4).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08158661B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-0571cadd15034c17b2d6f85711cbfdff |
| Source note | uspto-grants-2012_04 |