HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 178496601, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 178499305 | HCID 178499305 | — |
| Product | HCID 178496601 | HCID 178496601 | — |
Reaction Steps
The product from step IV (61 mg) was hydrolyzed with lithium hydroxide as described earlier (example 3, step VIII) to afford after column purification on silica gel (CH2Cl2-MeOH) 23 mg (39%) of 3-[(trans-4-methoxy-cyclohexyl)-(trans-4-methyl-cyclohexanecarbonyl)-amino]-5-(4-oxocyclohexyl)-thiophene-2-carboxylic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08158675B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-7f1bf7f5170049afa9b947187151924b |
| Source note | uspto-grants-2012_04 |