Ethanol → HCID 86645092, compound

HRID 1694534Notes

Reaction equation

HRID 1694534 reaction equation
[CH:1]1([CH:7]=[O:8])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.C(O)C.[S:12]([S:16]([O-:18])=[O:17])([O-:15])(=[O:14])=[O:13].[Na+].[Na+]>O>[S:12]([S:16]([OH:18])=[O:17])([OH:15])(=[O:14])=[O:13].[CH:1]1([CH:7]=[O:8])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

5

Reactant 3

HCID 702EthanolHCID 16275CyclohexanecarboxaldehydeHCID 656671Sodium Pyrosulfite

Product 1

HCID 86645092HCID 86645092, compoundYield 116.2%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

100 gms of cyclohexane carboxaldehyde was dissolved in 400 ml of industrial spirit (denatured ethanol) and a solution of sodium metabisulphite (95 gms) in water (150 ml) was added under stirring. The resulting precipitate was filtered and washed with industrial spirit and dried under vacuum at a temperature of about 50-60° C. to obtain 150 gms of the titled complex having 99.5% purity.

Workup

  1. filtrationThe resulting precipitate was filtered
  2. washwashed with industrial spirit
  3. customdried under vacuum at a temperature of about 50-60° C.

Sources & evidence

ORD record
ord-accd3f0b02f84476b019f750ad2e7e47
Source dataset
uspto-grants-2012_04
Patent number
US08158780B2

Reaction notes

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