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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1694697Generated: October 30, 2026

Dimethylformamide dimethyl acetal → HCID 67280479, compound

https://huagongshe.com/reaction/1694697

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethylformamide dimethyl acetalHCID 78373—
ReactantHCID 67280198HCID 67280198—
SolventTolueneHCID 1140—
ProductHCID 67280479HCID 67280479—

Reaction Conditions

Temperature100 °C

Reaction Steps

A mixture of the product from step (ii) (5.72 g) and dimethylformamide dimethyl acetal (3.5 ml) in toluene (50 ml) were heated at 100° C. for 12 h. The solvent was evaporated under reduced pressure to give an oil, 6.37 g.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08158820B2
Source datasetuspto-grants-2012_04
ORD IDord-bf319defa4164d12ad87ba081d583e13
Source noteuspto-grants-2012_04