Dimethylformamide dimethyl acetal → HCID 67280479, compound

HRID 1694697Notes

Reaction equation

HRID 1694697 reaction equation
[CH2:1]([O:8][C:9]1[CH:14]=[CH:13][C:12]([Cl:15])=[CH:11][C:10]=1[CH2:16][C:17]([CH3:19])=[O:18])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.CO[CH:22](OC)[N:23]([CH3:25])[CH3:24]>C1(C)C=CC=CC=1>[CH2:1]([O:8][C:9]1[CH:14]=[CH:13][C:12]([Cl:15])=[CH:11][C:10]=1/[C:16](=[CH:22]/[N:23]([CH3:25])[CH3:24])/[C:17](=[O:18])[CH3:19])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

4

Reactant 2

HCID 78373Dimethylformamide dimethyl acetalHCID 67280198HCID 67280198, compound

Product 1

HCID 67280479HCID 67280479, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Conditions

Temperature
100 °C

Procedure

A mixture of the product from step (ii) (5.72 g) and dimethylformamide dimethyl acetal (3.5 ml) in toluene (50 ml) were heated at 100° C. for 12 h. The solvent was evaporated under reduced pressure to give an oil, 6.37 g.

Workup

  1. customThe solvent was evaporated under reduced pressure
  2. customto give an oil, 6.37 g

Sources & evidence

ORD record
ord-bf319defa4164d12ad87ba081d583e13
Source dataset
uspto-grants-2012_04
Patent number
US08158820B2

Reaction notes

Loading…