Hydrochloric Acid → HCID 54587659, compound

Participants

Reaction Steps

A mixture of the product from step (v) (2.23 g), 1M aqueous sodium hydroxide (10 ml) and THF (20 ml) was stirred at RT for 3 h. The mixture was acidified with 2M hydrochloric acid, extracted with diethylether and the organics washed with water, dried, and evaporated under reduced pressure. The residue was recrystallised from ethylacetate/isohexane, yield 0.45 g.

Provenance & Evidence