反应详情

Sodium methanethiolate (5 g) was added to a solution of 4-fluoro-2-chloro-iodobenzene (18.3 g) and stirred for 20 h. The mixture was poured into water, extracted with ether, washed with brine, dried (MgSO4) and evaporated. Yield 18.5 g.

1. extractionextracted with ether
2. washwashed with brine
3. dry with materialdried (MgSO4)
4. customevaporated