HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pinacol → HCID 67279732, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pinacol | HCID 6425 | — |
| Reactant | 2-Benzyloxy-5-trifluoromethylphenylboronic acid | HCID 23005339 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 67279732 | HCID 67279732 | — |
Reaction Steps
Pinacol (1.82 g) was added to a solution of the product from example 32 step (ii) (4.54 g) in ether (40 ml) and stirred at RT for 20 h. The reaction was diluted with ether (100 ml), washed with brine, dried (MgSO4) and evaporated. Yield 5.7 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08158820B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-60768b1a4fa14a2bb7f9daacf7884501 |
| Source note | uspto-grants-2012_04 |