HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86654990, compound → HCID 86654989, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86654990 | HCID 86654990 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86654989 | HCID 86654989 | — |
Reaction Steps
10% Pd/C (0.15 g) was added to a solution of the product from example 165 step (ii) in EtOAc (20 ml) was hydrogenated at RT and 3 bar for 2 h. The mixture was filtered through celite and the filtrate evaporated to give the sub-title compound. Yield 1.4 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08158820B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-a8bafd334d894fc98beea8142499ba07 |
| Source note | uspto-grants-2012_04 |