反应详情

The product from step (iv) (0.564 g) was dissolved in 50% aqueous acetone (10 ml), sodium bicarbonate (0.94 g) added, followed by a solution of oxone (1.5 g) in water (ml) and stirred for 3 h. The reaction was quenched with aqueous sodium metabisulfite, extracted with EtOAc, washed with aqueous potassium carbonate, dried (Na2SO4) and evaporated to give the subtitle compound. Yield 0.32 g.

1. customThe reaction was quenched with aqueous sodium metabisulfite
2. extractionextracted with EtOAc
3. washwashed with aqueous potassium carbonate
4. dry with materialdried (Na2SO4)
5. customevaporated