HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 178436122, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Triethylsilane | HCID 12052 | — |
| Reactant | HCID 58951933 | HCID 58951933 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178436122 | HCID 178436122 | — |
Reaction Steps
Prepared in analogy to Example 57(e) from rac-(2-cyclopropyl-6-ethyl-phenyl)-(1-trityl-1H-imidazol-4-yl)-methanol, triethylsilane and trifluoroacetic acid in dichloromethane. Off-white crystalline solid. MS (ISP): 227.4 ([M+H]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08158668B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-37566e7a61a24584a4d1689252c67fd8 |
| Source note | uspto-grants-2012_04 |