HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid methylene chloride → HCID 57624519, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Reactant | HCID 67276668 | HCID 67276668 | — |
| Product | HCID 57624519 | HCID 57624519 | 111.7% |
Reaction Steps
Compound 30 (0.238 g) is treated with DCM-TFA (3 ml-1.5 ml) at 0° C. for 1 h. The volatiles are evaporated to dryness. Compound 31 (crude, 0.253 g) is obtained as white foam for use in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163693B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-a7e535b41ce041beb4655637bebe5186 |
| Source note | uspto-grants-2012_04 |