HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 17887686, compound → 3-(Difluoromethoxy)-β-oxobenzenepropanenitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 17887686 | HCID 17887686 | — |
| Reactant | HCID 67015924 | HCID 67015924 | — |
| Reactant | HCID 178418806 | HCID 178418806 | — |
| Product | 3-(Difluoromethoxy)-β-oxobenzenepropanenitrile | HCID 43123830 | — |
Reaction Steps
The product was prepared according to the general procedure for aminopyrazole synthesis (route A1 bis) from 3-difluoromethoxy-benzoic acid methyl ester (1.5 g, 7.4 mmol, 1.0 eq). The crude was precipitated by addition of aqueous HCl to give the product which was used directly for the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163729B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-5361f984f3ab4019976042004fa93322 |
| Source note | uspto-grants-2012_04 |