HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 49792921, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 66643884 | HCID 66643884 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 49792921 | HCID 49792921 | 16% |
Reaction Steps
As described for example 6, 5-(5-methyl-3-phenyl-isoxazol-4-ylmethoxy)-2H-pyrazole-3-carboxylic acid methyl ester (100 mg, 0.32 mmol) was converted, using ammonia in methanol instead of ethanolamine, to the title compound (15 mg, 16%), which was obtained as a white solid. MS: m/e=299.4 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163728B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-ac0caea75ebe48008e5fef737f6c2ef0 |
| Source note | uspto-grants-2012_04 |