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HRID1695587

反应详情

EQUATION

反应方程式

HRID 1695587 的结构方程式

REACTANTS

反应物

2
结构：COc1cccc2c1C(N)CC2
HCID18619881

7-Methoxy-2,3-dihydro-1H-inden-1-amine

C10H13NO

结构：CC(C)(C)[Si](C)(C)OCc1cc([N+](=O)[O-])ccc1N=C=S
HCID46855450

未命名化合物

PRODUCTS

生成物

1
结构：COc1cccc2c1C(NC1=Nc3ccc([N+](=O)[O-])cc3CO1)CC2
HCID178488350

未命名化合物

收率 73.4%

PROCEDURE

实验过程

Prepared from tert-butyl-(2-isothiocyanato-5-nitro-benzyloxy)-dimethyl-silane (Example C1) (3.89 g, 12.0 mmol; HPLC: 4.446 min) and the above described rac-7-methoxy-indan-1-ylamine (1.96 g, 12.0 mmol; HPLC 0.4 min) according to the procedure described for Example 1. Obtained the title compound as a yellow solid (2.99 g, 73%; HPLC 1.683 min), MS (ISP) m/e=340.1 [(M+H)+].