HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methoxyacetyl chloride → HCID 178496376, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methoxyacetyl chloride | HCID 96623 | — |
| Reactant | HCID 178507248 | HCID 178507248 | — |
| Product | HCID 178496376 | HCID 178496376 | 40.3% |
Reaction Steps
Prepared from rac-N2-(5-fluoro-indan-1-yl)-4H-benzo[d][1,3]oxazine-2,6-diamine (Example 11) (100 mg, 0.336 mmol) and methoxyacetyl chloride (34 ul, 0.370 mmol) according to the procedure described for Example 17. Obtained the title compound as a white solid (50 mg, 40%), MS (ISP) m/e=370.2 [(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163740B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-bf058083524d4be096025aa178537969 |
| Source note | uspto-grants-2012_04 |