2-Methoxyethylamine → HCID 178495942, compound

Participants

Reaction Steps

Prepared from the above described rac-2-chloro-N- [2-(6-fluoro-2,3-dihydro-benzofuran-3-ylamino)-4H-benzo[d][1,3]oxazin-6-yl]-acetamide (50 mg, 0.133 mmol, HPLC 1.056 min) and 2-methoxyethylamine (230 ul, 2.66 mmol) according to the procedure described for Example 3 step B. Obtained the title compound as a white solid (38 mg, 70%, HPLC 0.466 min 100%), MS (ISP) m/e=415.3 [(M+H)+].

Provenance & Evidence