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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1695617Generated: October 31, 2026

Acetic Anhydride → HCID 178488339, compound

https://huagongshe.com/reaction/1695617

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetic AnhydrideHCID 7918—
ReactantHCID 178488337HCID 178488337—
ProductHCID 178488339HCID 17848833988.2%

Reaction Steps

Prepared from rac-N2-(4-methoxy-2,3-dihydro-benzofuran-3-yl)-4H-benzo[d][1,3]oxazine-2,6-diamine (Example 6) (100 mg, 0.321 mmol) and acetic anhydride (60.7 ul, 0.642 mmol) according to the procedure described for Example 48. Obtained the title compound as a white solid (100 mg, 88%), MS (ISP) m/e=354.2 [(M+H)+].

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08163740B2
Source datasetuspto-grants-2012_04
ORD IDord-77a9244a3458402796370805071d4c57
Source noteuspto-grants-2012_04