HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 178488338, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 178488335 | HCID 178488335 | — |
| Product | HCID 178488338 | HCID 178488338 | 97% |
Reaction Steps
Prepared from rac-N2-(7-methoxy-indan-1-yl)-4H-benzo[d][1,3]oxazine-2,6-diamine (Example 10) (100 mg, 0.323 mmol) and acetic anhydride (61.1 ul, 0.646 mmol) according to the procedure described for Example 48. Obtained the title compound as a light brown foam (110 mg, 97%), MS (ISP) m/e=352.2 [(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163740B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-dff4b4ba18654db187a88a7177db0a06 |
| Source note | uspto-grants-2012_04 |