HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 178488348, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 178488342 | HCID 178488342 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178488348 | HCID 178488348 | 97.3% |
Reaction Steps
Prepared from the above described rac-2-chloro-N-[2-(7-methoxy-indan-1-ylamino)-4H-benzo[d][1,3]oxazin-6-yl]-acetamide (100 mg, 0.259 mmol) and morpholine (226 ul, 2.59 mmol) in acetonitrile (1 ml) according to the procedure described for Example 3 step B. Obtained the title compound as an off-white foam (110 mg, 97%), MS (ISP) m/e=437.2 [(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163740B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-49cbdaded86a40ae909280ecd5fe6464 |
| Source note | uspto-grants-2012_04 |